手机知网 App
24小时专家级知识服务
打 开
手机知网|搜索

5-芳基-3-二茂铁基二氢吡唑的合成及晶体结构

苏爱华;李恒东;高勇;袁耀锋

  A series of 5-aryl-3-ferrocenyl dihydropyrazole compounds were synthesized by using acetylferrocene.The structures of these compounds were characterized by IR,1H NMR spectra and MS.The crystal structure of compound 2a was determined by X-ray single crystal diffraction.The compound 2a belongs to the triclinic,space group P1,with a=10.203(6),b=10.447(7),c=11.557(8),α=96.80(3)°,β=116.05(2)°,γ=92.72(2)°,V=1092.1(12)3,Z=2,F(000)=412,Dc=1.353 g/cm3,μ=1.479 mm-1,and the final R1=0.0381,wR2=0.0834.……   
[关键词]:5-芳基-3-二茂铁基二氢吡唑;合成;晶体结构
[文献类型]:期刊
[文献出处]: 《化学研究与应用2010年02期
[格式]:PDF原版; EPUB自适应版(需下载客户端)