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N,N'-二(4-吡啶基)-3,4,9,10-苝四羧酸二酰亚胺的合成、表征及性能

刘福生;吉仁;吴敏;孙岳明

  The N,N -di(4-pyridyl)-3,4,9,10-perylene tetracarboxylic acid bisimide are obtained in good yield by reacting 4-aminopyridine with 3,4,9,10-perylenetetracarboxylic dianhydride in quinoline and anhydrous zinc acetate. In particular, N,N -di(4-pyridyl)-3,4,9,10-perylene tetracarboxylic acid bisimide has completely been studied, The structure of this compound was characterized by FT-IR spectra, UV-Vis(220-800nm) spectra, elemental analysis and 1H NMR. The result of structure analysis indicate that the compound which synthesized is N,N -di(4-pyridyl)-3,4,9,10-perylene tetracarboxylic acid bisimide. The thermal stability of this compound has been studied by the TG analysis. The data of TG analysis indicate that the compound is stable below 400℃. Hydrogen production from water splitting Using N,N -di(4-pyridyl)-3,4,9,10-perylene tetracarboxylic acid bisimide dye-sensitized Pt/TiO2 photocatalyst was investigated.……   
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