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  The structural and dynamics properties of molecules adsorbed in confined geometry have drawn much research attention in the past few decades.In this presentation,the methodologies and expediencies of utilizing appropriate adsorbates,such as xenon or phosphine oxides,as the probe molecules to characterize physical/chemical properties of porous adsorbents by means of ~(129)Xe and ~(31)p NMR spectroscopy will be discussed.……